Synthesis of cyclophanic chromium(0) bis(carbene) complexes
Organometallics, ISSN: 0276-7333, Vol: 20, Issue: 21, Page: 4304-4306
2001
- 28Citations
- 4Captures
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Article Description
Double Michael addition of 1,4- and 1,3-xylylene diamines and 1,5-diaminobutane to the bimetallic α,β-unsaturated alkoxychromium(0) carbene complex 4 produces in good to excellent yields the corresponding cyclophane bimetallic complexes 5-7 as single isomers. In contrast, the reaction with 1,4-diaminobutane produces a different cyclophane complex, 8, derived from a 1,2- + 1,4-addition process.
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