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Si-C attachment points during sol-gel synthesis of organosilicas from 2,8-bis-silylated Tröger's base as building block precursor

Journal of Materials Chemistry, ISSN: 0959-9428, Vol: 21, Issue: 24, Page: 8524-8527
2011
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The porous organosilica framework containing Tröger's base (TB) prepared by mild sol-gel synthesis from 2,8-bis-silylated TB precursor contains a mixture of two point attached TB and one point attached TB units, resulting from unexpected partial Si-C bond cleavage as demonstrated by Si MAS NMR spectroscopy and by selective chemo-desorption of the anchored organic part of the hybrid material. © 2011 The Royal Society of Chemistry.

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