Phosphine stabilized copper(i) complexes of dithiocarbamates and xanthates and their decomposition pathways
New Journal of Chemistry, ISSN: 1369-9261, Vol: 35, Issue: 12, Page: 2773-2780
2011
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- 16Captures
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Article Description
Phosphine stabilized compounds [Cu(i)(SCNEt)PR ] (1-3) (R = OMe, Me and Et, respectively) and [Cu(i)(SCOEt)PR] (4, 5), (R = OMe, and Me, respectively) have been prepared and characterised. The structures of compounds (1-3) were determined by X-ray single crystallography. The structures of all three compounds are based on centro-symmetric dimers which crystallise in the monoclinic space group P2/n with two [Cu(i)(SCNEt )PR] molecules per unit cell. The thermal decomposition of selected complexes was investigated by thermogravimetric, differential scanning calorimetry and gas chromatography with mass spectroscopy to understand the possible decomposition pathways. © 2011 The Royal Society of Chemistry and the Centre National de la Recherche Scientifique.
Bibliographic Details
Royal Society of Chemistry (RSC)
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