Dihalogen-templated synthesis of dodecanuclear silver dichalcogenophosphate clusters
CrystEngComm, ISSN: 1466-8033, Vol: 15, Issue: 13, Page: 6140-6143
2013
- 22Citations
- 8Captures
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Article Description
Dodecanuclear silver clusters, Ag(m-X)[EP(OEt)] (X = Br, I; E = S, Se), were isolated from the reaction of [Ag(CHCN)](PF), dichalcogenophosphate ammonium salts and halides in a common organic solvent. The Ag ring consists of two identical Ag units linked by intermolecular Ag–E bonds. The geometry of a Ag motif can be described as a bicapped tetrahedron, which is stabilized by a rare pentacoordinated bromine/iodine atom as well as five 1,1-dichalcogenophosphate ligands.
Bibliographic Details
Royal Society of Chemistry (RSC)
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