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Attenuated total reflectance infrared spectroelectrochemistry at a carbon particle electrode; Unmediated redox control of a [NiFe]-hydrogenase solution

Physical Chemistry Chemical Physics, ISSN: 1463-9076, Vol: 15, Issue: 19, Page: 7055-7059
2013
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Article Description

We report a versatile infrared spectroscopic method for studying redox chemistry of metalloproteins, and demonstrate for the first time electrochemically-induced changes to the active site of the regulatory [NiFe]-hydrogenase from Ralstonia eutropha. A carbon particle network working electrode allows control over a wide potential window without the need for solution mediators. © 2013 the Owner Societies.

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