Molecular, 1D and 2D assemblies from hexakis(3-pyridyloxy)cyclophosphazene containing 20-membered metallamacrocyclic motifs
Dalton Transactions, ISSN: 1477-9234, Vol: 45, Issue: 5, Page: 2273-2283
2016
- 25Citations
- 19Captures
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Metrics Details
- Citations25
- Citation Indexes25
- CrossRef25
- 23
- Captures19
- Readers19
- 19
Article Description
The coordination behaviour of hexakis(3-pyridyloxy)cyclophosphazene (L) towards divalent metal ions is described. The reaction of L with hydrated metal nitrates afforded [{NP(O-CHN-3)}{Zn(HO)(NO)}{Zn(HO)(NO)}][NO]·4nHO·nCHOH (1), [{NP(O-CHN-3)}{Zn(HO)(NO)}{Cu(NO)}][NO]·4nHO·nCHCN (2), [{NP(O-CHN-3)}{(NO)Cd-(μ-(NO)-Cd(NO)(μ-(NO)Cd(NO)}]·2nCHOH·3nHO (3), and [{NP(O-CHN-3)}{Cd(HO)(NO)}][NO]·9HO (4). 1 and 2 are one-dimensional coordination polymers while 3 is a two-dimensional coordination polymer. On the other hand 4 is a molecular metallamacrocycle. A common feature of 1-4 is the presence of a 20-membered dimetallamacrocyclic motif constructed through the involvement of a pair of cyclophosphazene ligands through their geminal pyridyloxy substituents. The P-N bond distances in L and its metal complexes 1-4 are nearly the same indicating the flexible nature of the coordination pyridyloxy arms present on the cyclophosphazene scaffold.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84956682024&origin=inward; http://dx.doi.org/10.1039/c5dt03537f; http://www.ncbi.nlm.nih.gov/pubmed/26687430; http://xlink.rsc.org/?DOI=C5DT03537F; http://pubs.rsc.org/en/content/articlepdf/2016/DT/C5DT03537F; https://xlink.rsc.org/?DOI=C5DT03537F; https://dx.doi.org/10.1039/c5dt03537f; https://pubs.rsc.org/en/content/articlelanding/2016/dt/c5dt03537f
Royal Society of Chemistry (RSC)
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