Online quantitative mass spectrometry for the rapid adaptive optimisation of automated flow reactors
Reaction Chemistry and Engineering, ISSN: 2058-9883, Vol: 1, Issue: 1, Page: 96-100
2016
- 109Citations
- 133Captures
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Example: if you select the 1-year option for an article published in 2019 and a metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019. If you select the 3-year option for the same article published in 2019 and the metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019, 2018 and 2017.
Citation Benchmarking is provided by Scopus and SciVal and is different from the metrics context provided by PlumX Metrics.
Article Description
An automated continuous reactor for the synthesis of organic compounds, which uses online mass spectrometry (MS) for reaction monitoring and product quantification, is presented. Quantitative and rapid MS monitoring was developed and calibrated using HPLC. The amidation of methyl nicotinate with aqueous MeNH2 was optimised using design of experiments and a self-optimisation algorithm approach to produce >93% yield.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84979286008&origin=inward; http://dx.doi.org/10.1039/c5re00083a; http://xlink.rsc.org/?DOI=C5RE00083A; http://pubs.rsc.org/en/content/articlepdf/2016/RE/C5RE00083A; https://xlink.rsc.org/?DOI=C5RE00083A; https://dx.doi.org/10.1039/c5re00083a; https://pubs.rsc.org/en/content/articlelanding/2016/re/c5re00083a
Royal Society of Chemistry (RSC)
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