Efficient synthesis of carborane azo derivatives and their reactivity
Dalton Transactions, ISSN: 1477-9234, Vol: 46, Issue: 5, Page: 1585-1592
2017
- 21Citations
- 8Captures
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Article Description
An iridium(iii)-catalyzed C-N-bond-forming direct synthesis of carborane azo derivatives was developed. The reaction of o-carborane monocarboxylate with aryldiazonium salt in the presence of a catalytic amount of [Cp∗IrCl] and NaOAc in CHCN at 80 °C gave the corresponding carborane azo derivative in good yield. A series of cyclometalated iridium/rhodium complexes that contain Cp∗M-B (M = Ir, Rh) bonds, and are stabilised by the intramolecular coordination of nitrogen donors, were successfully isolated and structurally characterised.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85011116130&origin=inward; http://dx.doi.org/10.1039/c6dt04550b; http://www.ncbi.nlm.nih.gov/pubmed/28091648; http://xlink.rsc.org/?DOI=C6DT04550B; http://pubs.rsc.org/en/content/articlepdf/2017/DT/C6DT04550B; https://xlink.rsc.org/?DOI=C6DT04550B; https://dx.doi.org/10.1039/c6dt04550b; https://pubs.rsc.org/en/content/articlelanding/2017/dt/c6dt04550b
Royal Society of Chemistry (RSC)
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