Synthesis, characterization, crystal structure, electrochemical, solvatochromic and biological investigation of novel N4 and N3 type Cu(II) Schiff base complexes
New Journal of Chemistry, ISSN: 1369-9261, Vol: 41, Issue: 21, Page: 12554-12561
2017
- 8Citations
- 11Captures
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Article Description
In the present study, three novel Cu(ii) Schiff base complexes [CuL](ClO), [CuL′Cl] and [CuL′(NO)] (L: N,N′-bis(2-pyridinylmethylene)-1,2-diphenylethylenediamine and L′: N-(2-pyridinylmethylene)-1,2-diphenylethylenediamine) were synthesized and characterized using infrared spectroscopy, elemental analysis, conductivity measurements and X-ray crystallography. The crystal structure of the [CuL′(NO)] and [CuL′Cl] complexes were determined by X-ray crystallography. However, suitable single crystals for [CuL](ClO) could not be obtained. The complexes were assessed to determine their thermal, electrochemical and biological behaviors and electronic absorption. Among the complexes, only the [CuL](ClO) complex showed solvatochromic properties in various solvents. The antibacterial activities of these complexes were evaluated in Muller-Hinton broth against Staphylococcus aureus, Escherichia coli and Enterococcus faecalis using the serial dilution technique at concentrations ranging from 2 to 0.0625 mg mL. The data demonstrates that the complexes were bacteriostatic agents that inhibit bacterial growth, but had no bactericidal properties.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85032586947&origin=inward; http://dx.doi.org/10.1039/c7nj02187a; https://xlink.rsc.org/?DOI=C7NJ02187A; http://xlink.rsc.org/?DOI=C7NJ02187A; http://pubs.rsc.org/en/content/articlepdf/2017/NJ/C7NJ02187A; https://dx.doi.org/10.1039/c7nj02187a; https://pubs.rsc.org/en/content/articlelanding/2017/nj/c7nj02187a
Royal Society of Chemistry (RSC)
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