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A regio- and stereoselective Heck-Matsuda process for construction of γ-aryl allylsulfonyl fluorides

RSC Advances, ISSN: 2046-2069, Vol: 12, Issue: 30, Page: 19402-19405
2022
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Article Description

A highly efficient regio- and stereoselective Heck-Matsuda method was developed employing aryl diazoniums and allylsulfonyl fluorides for the construction of a class of novel γ-aryl allylsulfonyl fluorides in the presence of Pd(OAc) and PPh. The method features excellent regio- and stereoselectivity (up to 100% E-selectivity), broad substrate scope and mild reaction conditions. Further application of γ-aryl allylsulfonyl fluoride in SuFEx reactions was achieved to provide their corresponding sulfonates and sulfonamides in excellent yields.

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