Mechano-chemical Synthesis of NaAlH: Optimization of Reaction Conditions
MATEC Web of Conferences, ISSN: 2261-236X, Vol: 67
2016
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Conference Paper Description
NaAlH was mechano-chemically synthesized with high energy ball-milling method. The effect of synthesis conditions such as milling time, H pressure, chloride catalysts, and solvents was investigated to enhance the synthesis of NaAlH. Among the chloride catalysts, TiCl showed the highest H pressure decrease which means the highest NaH conversion to NaAlH. Furthermore, when the NaAlH was synthesized with THF solvent, it exhibited the higher H pressure decrease than that of sample prepared without THF solvent. This is mainly due to the synergy effect of TiCl catalyst and THF solvent.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84982095637&origin=inward; http://dx.doi.org/10.1051/matecconf/20166706064; http://www.matec-conferences.org/10.1051/matecconf/20166706064; http://www.matec-conferences.org/10.1051/matecconf/20166706064/pdf; https://dx.doi.org/10.1051/matecconf/20166706064; https://www.matec-conferences.org/articles/matecconf/abs/2016/30/matecconf_smae2016_06064/matecconf_smae2016_06064.html
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