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3,3-dimethyl-cis-9a,13a-diphenyl-2,3,9a,11,12,13a-hexahydro-1H-benzo[h][1, 4]dioxino[2′,3′:5,6][1,4]dioxino[2,3-f]chromene

Acta Crystallographica Section E: Structure Reports Online, ISSN: 1600-5368, Vol: 69, Issue: 9, Page: o1487-8
2013
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Article Description

In the title dihydrodioxin, CHO, the dioxane ring has a chair conformation, whereas each of the pyran and dioxine rings has an envelope conformation with methylene and quaternary C atoms, respectively, being the flap atoms. The phenyl rings are cis and form a dihedral angle of 82.11 (10)°. The molecular structure is stabilized by C - H⋯O contacts. In the crystal packing, supramolecular layers parallel to (101) are sustained by C - H⋯π interactions. © 2013 Bernardes et al.

Bibliographic Details

Bauer O. Bernardes; Aurelio B. Buarque Ferreira; James L. Wardell; Solange M. S. V. Wardell; José C. Netto-Ferreira; Edward R. T. Tiekink

International Union of Crystallography (IUCr)

Chemistry; Materials Science; Physics and Astronomy

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