C - I⋯N short contacts as tools for the construction of the crystal packing in the crystal structure of 3,3′-(ethane-1,2-diyl)bis(6-iodo-3,4-dihydro-2H-1,3-benzoxazine)
Acta Crystallographica Section E: Crystallographic Communications, ISSN: 2056-9890, Vol: 73, Issue: Pt 5, Page: 664-666
2017
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Article Description
The asymmetric unit of the title compound, CHINO, consists of one half-molecule, completed by the application of inversion symmetry. The molecule adopts the typical structure for this class of bis-benxozazines, characterized by an anti orientation of the two benzoxazine rings around the central C - C bond. The oxazinic ring adopts a half-chair conformation. In the crystal, molecules are linked by C - I⋯N short contacts [I⋯N = 3.378(2)Å], generating layers lying parallel to the bc plane.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85019028682&origin=inward; http://dx.doi.org/10.1107/s2056989017005047; http://www.ncbi.nlm.nih.gov/pubmed/28529771; http://scripts.iucr.org/cgi-bin/paper?S2056989017005047; http://journals.iucr.org/e/issues/2017/05/00/hb7668/hb7668.pdf; https://journals.iucr.org/paper?S2056989017005047; https://dx.doi.org/10.1107/s2056989017005047; https://journals.iucr.org/e/issues/2017/05/00/hb7668/index.html
International Union of Crystallography (IUCr)
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