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Copper(II) alkyl- and benzylnitrosohydroxylaminates as precursors for the synthesis of copper(I) oxide micro- and nanoparticles of various morphologies

Inorganic Materials, ISSN: 1608-3172, Vol: 50, Issue: 11, Page: 1093-1098
2014
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Article Description

We describe the thermal decomposition of a number of copper(II) alkyl- and benzylnitrosohy-droxylaminates via thermostating in polyethylene glycol and 2-dodecyl-1H-imidazole for various lengths of time. This process is shown to lead to the formation of copper(I) oxide nanoparticles, which have been characterized by X-ray diffraction and electron spectroscopy. The starting copper(II) nitrosohydroxylaminates have been characterized by thermogravimetry.

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