Synthesis, properties, and crystal structure of the tin(IV) complex with N-(2-hydroxyethyl)ethylenediaminetriacetic acid [Sn(μ-Hedtra)(μ-OH) SnCl(HO)] · 3HO
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, ISSN: 1070-3284, Vol: 39, Issue: 7, Page: 505-509
2013
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Article Description
The binuclear tin(IV) complex with N-(2-hydroxyethyl)ethylenediamine-N, N′,N′-triacetic acid (HHedtra) is synthesized. The compound is characterized by elemental analysis, thermogravimetry, and IR spectroscopy. An X-ray diffraction analysis of complex Sn(μ-Hedtra)(μ-OH) SnCl(HO)] · 3HO (I) is carried out. Structure I is formed by the binuclear complexes and molecules of water of crystallization. One of the tin atoms coordinates six "active" sites Hedtra (the alcohol branch is deprotonated and forms a bridge between two tin atoms) and the bridging hydroxo group. The polyhedron is a pentagonal bipyramid. The octahedral environment of the second tin atom is formed by two bridging oxygen atoms, three chlorine atoms (fac isomer), and a coordination water molecule. © 2013 Pleiades Publishing, Ltd.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84880228165&origin=inward; http://dx.doi.org/10.1134/s1070328413070075; http://link.springer.com/10.1134/S1070328413070075; http://link.springer.com/content/pdf/10.1134/S1070328413070075; http://link.springer.com/content/pdf/10.1134/S1070328413070075.pdf; http://link.springer.com/article/10.1134/S1070328413070075/fulltext.html; https://dx.doi.org/10.1134/s1070328413070075; https://link.springer.com/article/10.1134/S1070328413070075
Pleiades Publishing Ltd
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