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Neutral and monocationic dinuclear (carbonyl)(cyclopentadienyl) (phenylchalcogenate) iron complexes of the general formulas [(RC H)Fe(CO)EPh] and [(RCH )Fe(CO)EPh]PF (E = S or Te; R = H or Me): Synthesis, molecular structures, and EPR spectra

Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, ISSN: 1070-3284, Vol: 39, Issue: 12, Page: 822-828
2013
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Heating of the compounds (RCH)Fe(CO) TePh (R = H (I) and Me (II)) in heptane afforded the dinuclear complexes [(RCH)Fe(CO)TePh] (III and IV, respectively). By oxidation with FcPF, these complexes were transformed into the paramagnetic cationic complexes [(RC H)Fe(CO)TePh]PF (Vand VI, respectively). Structures III-V and [(CH)Fe(CO)SPh] PF (VII) were characterized by X-ray diffraction. © Pleiades Publishing, Ltd., 2013.

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