Electrochemical properties and fluorination of cyclopropane derivatives bearing arylthio groups
Journal of the Electrochemical Society, ISSN: 1945-7111, Vol: 167, Issue: 15
2020
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- 5Captures
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Article Description
Electrochemical analyses of phenylthiocyclopropane derivatives and bis(arylthio)cyclopropanes were comparatively studied by cyclic voltammetric measurements. Based on the substituent effects on their oxidation potentials, a cyclopropane ring was confirmed to have a double bond system as reported. Anodic fluorination of phenylthiocyclopropanes resulted in the formation of sulfoxide and/or ring opening fluorinated products while 1,1-bis(arylthio)cyclopropanes afforded mainly desulfurizative monofluorinated cyclopropanes and sulfoxides together with ring opening fluorinated products. This is the first successful electrochemical fluorination of a cyclopropane ring.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85092483066&origin=inward; http://dx.doi.org/10.1149/1945-7111/abb83b; https://iopscience.iop.org/article/10.1149/1945-7111/abb83b; https://dx.doi.org/10.1149/1945-7111/abb83b; https://validate.perfdrive.com/fb803c746e9148689b3984a31fccd902/?ssa=56c8345d-10d3-435d-86f3-d450bf36c809&ssb=04006254562&ssc=https%3A%2F%2Fiopscience.iop.org%2Farticle%2F10.1149%2F1945-7111%2Fabb83b&ssi=366bcb3d-8427-45b9-ad25-d2dece04c7d5&ssk=support@shieldsquare.com&ssm=179651823751861591150878648264360629&ssn=115f1a166c07aed80595b48ae2eec3f3554617f9ea44-4e1f-4e35-bca792&sso=2e5d615e-f9d9f87a371f8dad4962bb2102aac127d2cb8f2fa61985f7&ssp=16693272851719367955171976047792016&ssq=08806368648330040145205699943311239980871&ssr=NTIuMy4yMTcuMjU0&sst=com.plumanalytics&ssu=&ssv=&ssw=&ssx=eyJfX3V6bWYiOiI3ZjYwMDBjMGI2MzM1NC00OGRkLTRjNTUtODVmZS00NzZmMjgxYzE5ZDgxNzE5MzA1Njk5NDA1NDgwNzg0NTE2LTcwOGQ3YTRiZDE0MmNiZmUxMTUwNzgiLCJ1em14IjoiN2Y5MDAwMWUxYTVkMGQtYjRlNi00ZTQ0LWFmYTgtNzUxMTFmZjg0ZDlmNi0xNzE5MzA1Njk5NDA1NDgwNzg0NTE2LTBhZjBjYWQwMzZkMWFjYWQxMTUwNzUiLCJyZCI6ImlvcC5vcmcifQ==
The Electrochemical Society
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