Flow-injection preconcentration of chloramphenicol using molecularly imprinted polymer for HPLC determination in environmental samples
Journal of Automated Methods and Management in Chemistry, ISSN: 1463-9246, Vol: 2011, Page: 143416
2011
- 12Citations
- 24Captures
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Metrics Details
- Citations12
- Citation Indexes12
- 12
- CrossRef9
- Captures24
- Readers24
- 24
Article Description
The residue of antibiotic chloramphenicol (CAP) is important issue for food quality control and also for the environmental monitoring. It is banned for use in food-producing animals and has very limited use in human medicine, because of its severe impact on human health. Determination of trace level of CAP in environmental samples requires a very sensitive analytical method and efficient preconcentration procedure. CAP can be efficiently preconcentrated in flow-injection system using flow-through reactor packed with molecularly imprinted polymer (MIP), but determination of CAP in eluate from MIP requires the application of chromatographic separation, which was made in reversed-phase HPLC system with UV detection. In optimized conditions the limit of detection for 100mL sample in HPLC with offline preconcentration on MIP was evaluated as 0.66mg/L. In hyphenated FIA-HPLC system with zone sampling the LOD for developed method was evaluated as 15ng/L, which indicates the possibility of using it for analysis of environmental samples. Copyright © 2011 Damian Kowalski et al.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=79959258372&origin=inward; http://dx.doi.org/10.1155/2011/143416; http://www.ncbi.nlm.nih.gov/pubmed/21584273; http://www.hindawi.com/journals/jamc/2011/143416/; https://dx.doi.org/10.1155/2011/143416; https://www.hindawi.com/journals/jamc/2011/143416/
Hindawi Limited
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