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Flash spark plasma sintering of ZrTiC solid solution

Journal of the Ceramic Society of Japan, ISSN: 1348-6535, Vol: 129, Issue: 9, Page: 574-578
2021
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Article Description

ZrTiC (x = 0, 0.2, 0.4, 0.6, 0.8, 1) solid solution ceramics were fabricated by flash spark plasma sintering (FSPS). The phase composition, microstructure, and mechanical property of the flash sintered ceramics were investigated. The results showed that the composition of ZrTiC solid solution plays a key role on the densification of the ceramics. A high relative density (98.6 %) and hardness (>20 GPa) was achieved in a solid solution composition of ZrTiC. The unique in-situ high temperature, fast cooling rate, and mold-free sintering in the FSPS sintering process leads to the formation of gradient microstructure in ZrTiC solid solution, where the corresponding density and hardness show gradient distribution characteristics.

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