Novel Magnetite (FeO)-Methylcellulose Nanocomposites Synthesized Using the Reverse Co-Precipitation Approach
Journal of Composites Science, ISSN: 2504-477X, Vol: 8, Issue: 7
2024
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J. Compos. Sci., Vol. 8, Pages 282: Novel Magnetite (Fe3O4)-Methylcellulose Nanocomposites Synthesized Using the Reverse Co-Precipitation Approach
J. Compos. Sci., Vol. 8, Pages 282: Novel Magnetite (Fe3O4)-Methylcellulose Nanocomposites Synthesized Using the Reverse Co-Precipitation Approach Journal of Composites Science doi: 10.3390/jcs8070282 Authors: Ashraf
Article Description
A simple approach was used to create FeO-methylcellulose (MC) nanocomposites, which were then analyzed using XRD, FTIR, and FE-SEM to determine their structure. The effective factors for enhancing the ratio of magnetite NPs in the samples were investigated using RTFM and optical absorbance. FeO was synthesized utilizing the reverse co-precipitation technique and magnetic characteristics. FeO/MC nanocomposites with magnetite/MC weight ratios of 0, 0.07, 0.15, and 0.25 have been developed. The diffraction pattern of magnetite is well indexed in accordance with the spinal reference pattern of FeO (space group: R¯3m), as confirmed by the Rietveld analysis of XRD data of magnetite NPs with an average crystallite size of 50 nm. Magnetite’s insertion into the MC network causes a red shift in the band gap energy (E) as the weight percentage of magnetite nanoparticles in the samples rises. The MC, MC-7, MC-15, and MC-25 samples have E values of 5.51, 5.05, 2.84, and 2.20 eV, respectively.
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